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Fragmentation of coal and improved dispersion of liquefaction catalysts using ionic liquids

Başlık çevirisi mevcut değil.

  1. Tez No: 401903
  2. Yazar: RUVEYDA ÇETİNER
  3. Danışmanlar: DR. JONATHAN P. MATHEWS, DR. PAUL C. PAINTER
  4. Tez Türü: Yüksek Lisans
  5. Konular: Enerji, Maden Mühendisliği ve Madencilik, Energy, Mining Engineering and Mining
  6. Anahtar Kelimeler: Belirtilmemiş.
  7. Yıl: 2011
  8. Dil: İngilizce
  9. Üniversite: The Pennsylvania State University
  10. Enstitü: Yurtdışı Enstitü
  11. Ana Bilim Dalı: Belirtilmemiş.
  12. Bilim Dalı: Belirtilmemiş.
  13. Sayfa Sayısı: 113

Özet

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Özet (Çeviri)

Coal has been utilized for coal-to-liquid fuels and coal-to-chemical industries both historically in South Africa and recently in China. Abundant bituminous and low-rank coal reserves in the US make them potential sources of an alternative to the oil derived petrochemical industry. Consequently, it is desirable to evaluate new processes for conversion of solid coal-to-clean liquid fuels. One such approach may utilize ionic liquids, a relatively new addition to industrial processing. Ionic liquids can engage in a wide range of intermolecular interactions with coal that may result in alternative approaches to fragment, disperse, and dissolve coal. They have negligible vapor pressure, are non-flammable, and would be easier to handle than traditional solvent approaches. The goal of this work was to explore the ability of certain ionic liquids (ILs) to fragment, disperse and partially dissolve coals in order to allow a better contact with micron size catalyst particles prior to direct coal liquefaction. Attention was focused primarily on the ionic liquid 1-butyl-3-methylimidazolium chloride [bmim][Cl] and the coals studied were Illinois No.6 bituminous coal and Power River Basin subbituminous coal. Coal was mixed with ILs in a ratio of 10% by weight at 100 ºC in an oil bath without agitation. Fragmentation was evaluated by optical microscopy.It was found that the IL [bmim][Cl] fragmented and dispersed Illinois No. 6 coal to a remarkable extent. Optical microscopy demonstrated that the -100 mesh particles were reduced in size to

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