Developing of the hybrid material for remove the Cu (II) and Co (II) ions from the drinking and waste waters
Hibrit malzemenin gelişiminden Cu (II) ve Co (II) iyonlarının atık su ve içme suyunun çözülmesine geliştirilmesi
- Tez No: 465094
- Danışmanlar: Assist. Prof. Dr. MUHARREM KARABÖRK
- Tez Türü: Yüksek Lisans
- Konular: Kimya, Chemistry
- Anahtar Kelimeler: Heavy metals, Multi-Walled Carbon Nanotubes, Silanization, Hybrid Material, Purification, Heavy metals, Multi-Walled Carbon Nanotubes, Silanization, Hybrid Material, Purification
- Yıl: 2017
- Dil: İngilizce
- Üniversite: Kahramanmaraş Sütçü İmam Üniversitesi
- Enstitü: Fen Bilimleri Enstitüsü
- Ana Bilim Dalı: Kimya Ana Bilim Dalı
- Bilim Dalı: Belirtilmemiş.
- Sayfa Sayısı: 85
Özet
DEVELOPING OF THE HYBRID MATERIAL FOR REMOVE THE CU (II) AND CO (II) IONS FROM THE DRINKING AND WASTE WATERS (M.Sc) Thesis Idrees Salim Khalo ABSTRACT Multi-walled carbon nanotubes (MWCNTs) show a unique impact on the fast adsorption and rapid removal of harmful impurities from the aqueous source due to it has unique properties such as mechanical strength, electrical and thermal conductivity. MWCNTs were modified as hybrid a sorbent and used as purification for the removal of Copper(II) and Cobalt(II) from aqueous solutions. As-received MWCNTs was modified in three treatments oxidation (H2SO4 /H2O2) according to Hummer method, silanization [(3-aminopropyl) triethoxysilane] (APTES) and Schiff base (3, 5-dichloro salicylaldehyde) to introduce onto the surface of the MWCNTs carboxyl, silane and aldehyde groups respectively. Multifunctionality MWCNTs has been characterized by Fourier Transform Infrared (FT-IR) Spectroscopy, Ultraviolet–Visible Spectroscopy (Uv-vis), Thermo Gravimetric (TGA) Analysis, Raman Spectra, Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), Energy Dispersive X-ray Spectrum (EDX), and ICP-OES Analysis. Additionally adsorption parameters such as pH, contact time, temperature, and initial concentrations were optimized.
Özet (Çeviri)
DEVELOPING OF THE HYBRID MATERIAL FOR REMOVE THE CU (II) AND CO (II) IONS FROM THE DRINKING AND WASTE WATERS (M.Sc) Thesis Idrees Salim Khalo ABSTRACT Multi-walled carbon nanotubes (MWCNTs) show a unique impact on the fast adsorption and rapid removal of harmful impurities from the aqueous source due to it has unique properties such as mechanical strength, electrical and thermal conductivity. MWCNTs were modified as hybrid a sorbent and used as purification for the removal of Copper(II) and Cobalt(II) from aqueous solutions. As-received MWCNTs was modified in three treatments oxidation (H2SO4 /H2O2) according to Hummer method, silanization [(3-aminopropyl) triethoxysilane] (APTES) and Schiff base (3, 5-dichloro salicylaldehyde) to introduce onto the surface of the MWCNTs carboxyl, silane and aldehyde groups respectively. Multifunctionality MWCNTs has been characterized by Fourier Transform Infrared (FT-IR) Spectroscopy, Ultraviolet–Visible Spectroscopy (Uv-vis), Thermo Gravimetric (TGA) Analysis, Raman Spectra, Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), Energy Dispersive X-ray Spectrum (EDX), and ICP-OES Analysis. Additionally adsorption parameters such as pH, contact time, temperature, and initial concentrations were optimized.
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